2-Bromo-6-nitrobenzoic acid synthesis
- Product Name:2-Bromo-6-nitrobenzoic acid
- CAS Number:38876-67-4
- Molecular formula:C7H4BrNO4
- Molecular Weight:246.01
603-62-3
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38876-67-4
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Yield:-
Steps:
Multi-step reaction with 3 steps
1.1: sodium hydroxide / water / 2 h / 0 °C / Inert atmosphere
2.1: sodium hydroxide; bromine / water / 0.75 h / 0 - 45 °C / Inert atmosphere
3.1: sodium nitrite; hydrogen bromide; acetic acid / water / 0 °C / Inert atmosphere
3.2: 0 - 65 °C / Inert atmosphere
References:
Chu, John C. K.;Dalton, Derek M.;Rovis, Tomislav [Journal of the American Chemical Society,2015,vol. 137,# 13,p. 4445 - 4452]
55289-35-5
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38876-67-4
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50573-74-5
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$16.00/250mg
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65911-46-8
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38876-67-4
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