2-Bromo-6-fluoropyridine synthesis
- Product Name:2-Bromo-6-fluoropyridine
- CAS Number:144100-07-2
- Molecular formula:C5H3BrFN
- Molecular Weight:175.99
626-05-1
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$9.00/10g
144100-07-2
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$10.00/5g
Yield:-
Reaction Conditions:
with potassium fluoride
Steps:
35 Preparation by method B:
100 g (422.10 mmol) of 2,6-dibromopyridine, 36.79 g (633.15 mmol) of potassium fluoride and 11.16 g of 18-crown-6 are heated in a distillation apparatus 190° C. under vacuum (200 mbar), and the reaction product is distilled off. Repeated purification by distillation gives 43.90 g of 2-bromo-6-fluoropyridine having a boiling point of 70° C. at 15 mbar. STR66
References:
US5630962,1997,A
21203-78-1
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$32.00/100mg
144100-07-2
239 suppliers
$10.00/5g
109-04-6
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$6.00/25g
372-48-5
383 suppliers
$5.00/5g
144100-07-2
239 suppliers
$10.00/5g
109-04-6
530 suppliers
$6.00/25g
144100-07-2
239 suppliers
$10.00/5g