2-Bromo-4-methylbenzaldehyde synthesis
- Product Name:2-Bromo-4-methylbenzaldehyde
- CAS Number:824-54-4
- Molecular formula:C8H7BrO
- Molecular Weight:199.04
824-53-3
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$130.00/1g
824-54-4
137 suppliers
$12.00/1g
Yield:824-54-4 83%
Reaction Conditions:
with triphenylmethyl alcohol;iron(III) chloride hexahydrate at 55; for 1 h;Microwave irradiation;
Steps:
General procedures for the synthesis of benzaldehydes
General procedure: The benzyl alcohols substrates (1a-1p) (0.2mmol), FeCl3·6H2O (0.002mmol, 5.4mg) and triphenylmethanol 2 (0.2mmol, 52mg) were mixed in a dried vessel. Then the reaction was irradiated under the microwave at 55°C for 1h. The crude mixture was purified by a flash column chromatography to afford the benzaldehydes (4a-4p).
References:
Wang, Xiaoyu;Du, Chuan;Shi, Hui;Pang, Yadong;Jin, Shengfei;Hou, Yuqian;Wang, Yanshi;Peng, Xiaoshi;Xiao, Jianyong;Liu, Yang;Liu, Yongxiang;Cheng, Maosheng [Tetrahedron,2015,vol. 71,# 38,p. 6744 - 6748]
938461-09-7
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824-54-4
137 suppliers
$12.00/1g
42872-73-1
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$15.00/5g
824-54-4
137 suppliers
$12.00/1g
