ChemicalBook CAS DataBase List 2-BIPHENYLYL ISOCYANATE

2-BIPHENYLYL ISOCYANATE synthesis

6synthesis methods

Product Name:2-BIPHENYLYL ISOCYANATE
CAS Number:17337-13-2
Molecular formula:C13H9NO
Molecular Weight:195.22

90-41-5 Synthesis

90-41-5
353 suppliers
$16.00/5g

101-68-8 Synthesis

101-68-8
260 suppliers
$13.00/25g

17337-13-2
113 suppliers
$44.00/5g

Yield:17337-13-2 203.2 g

Reaction Conditions:

at 140 - 160; for 0.833333 h;Large scale;

Steps:

Preparation of 2-biphenyl isocyanate

Preparation of 2-biphenyl isocyanate
A three-neck flask with dropping funnel, precision glass stirrer and distillation attachment was initially charged with 1500 g of Desmodur 2460M and heated to 140° C.
Then, within 50 minutes, 243.7 g of 2-aminobiphenyl were added and the reaction temperature was kept below 160° C.
Subsequently, the product was distilled off under high vacuum (about 0.03 mbar), and 203.2 g of 2-biphenyl isocyanate, a clear liquid, were obtained.

References:

US2017/362165,2017,A1 Location in patent:Paragraph 0188

32315-10-9 Synthesis