2-Amino-4-(methylamino)-1,3,5-triazine synthesis
- Product Name:2-Amino-4-(methylamino)-1,3,5-triazine
- CAS Number:58228-69-6
- Molecular formula:C4H7N5
- Molecular Weight:125.13
Yield:58228-69-6 106 mg
Reaction Conditions:
in tetrahydrofuran at 20; for 0.166667 h;
Steps:
1.A Step A:
The mixture of 4-chloro-1, 3, 5-triazin-2-amine (200 mg, 1.5 mmol) in MeNH2/THF (2mol/L, 10 mL) was stirred at r.t. for 10 min. The mixture was concentrated in vacuo, and the residue was purified by flash chromatography (DCM/MeOH 10/1) to afford the desired product as a white solid. (106 mg) . LC-MS: m/z 125.9 (M+H) +.
References:
AGIOS PHARMACEUTICALS, INC.;TRAVINS, Jeremy, M.;KONTEATIS, Zenon, D.;SUI, Zhihua;YE, Zhixiong WO2018/39972, 2018, A1 Location in patent:Page/Page column 181
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