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95216-09-4

2,6-Dimethylterephthalonitrile synthesis

4synthesis methods
-

Yield:-

Steps:

Multi-step reaction with 3 steps
1: 40 percent / NaOH / benzene; aq. ethanol; 2-methyl-propan-2-ol / 8 h / Heating
2: 85 percent / 85percent H2O2 / CHCl3; acetic acid / 42 h / 20 °C
3: 6 mg / 480 - 500 °C / 0 - 0.01 Torr

References:

Staab, Heinz A.;Schanne, Lothar;Krieger, Claus;Taglieber, Volker [Chemische Berichte,1985,vol. 118,# 3,p. 1204 - 1229]