2-(4-CHLORO-PHENYL)-OXAZOLE-4-CARBALDEHYDE synthesis
- Product Name:2-(4-CHLORO-PHENYL)-OXAZOLE-4-CARBALDEHYDE
- CAS Number:59398-91-3
- Molecular formula:C10H6ClNO2
- Molecular Weight:207.61
![[2-(4-CHLORO-PHENYL)-OXAZOL-4-YL]-METHANOL](/CAS/GIF/22087-22-5.gif)
22087-22-5
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Yield:-
Reaction Conditions:
with manganese(IV) oxide in dichloromethane at 25 - 30; for 18 h;Inert atmosphere;
Steps:
General procedure for the synthesis of Q4
General procedure for the synthesis of 04A mixture of Q3 (1.49 g, 7.13 mmol) and Mn02 (6.20 g, 71.3 mmol) in DCM (65 mL) was stilTed under N2 atmosphere at 25-30 °C for 18 hours. The mixture was filtered and the filter cake was washed with DCM (10 mL x 2), the filtrate was concentrated under reduced pressure to dryness to afford Q4.
References:
WO2016/16421,2016,A1 Location in patent:Page/Page column 54; 55
300800-07-1
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104-88-1
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$5.00/25g
59398-91-3
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