2,4-BIS(BENZYLOXY)PYRIMIDINE-5-BORONIC ACID synthesis
- Product Name:2,4-BIS(BENZYLOXY)PYRIMIDINE-5-BORONIC ACID
- CAS Number:70523-24-9
- Molecular formula:C18H17BN2O4
- Molecular Weight:336.15
41244-53-5
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$60.00/50mg
70523-24-9
95 suppliers
$63.00/500mg
Yield: 95%
Reaction Conditions:
Stage #1:5-bromo-2,4-bis(benzyloxy)pyrimidine with n-butyllithium;Triisopropyl borate in tetrahydrofuran;hexane;toluene at 20; for 18 h;
Stage #2: with hydrogenchloride in tetrahydrofuran;hexane;toluene
References:
Seley, Katherine L.;Salim, Samer;Zhang, Liang;O'Daniel, Peter I. [Journal of Organic Chemistry,2005,vol. 70,# 5,p. 1612 - 1619]