2,3-DIHYDRO-1H-BENZ[DE]ISOQUINOLINE synthesis
- Product Name:2,3-DIHYDRO-1H-BENZ[DE]ISOQUINOLINE
- CAS Number:22817-26-1
- Molecular formula:C12H11N
- Molecular Weight:169.22
![1H-Benz[de]isoquinoline, 2,3-dihydro-2-(phenylmethyl)-](/CAS/20210305/GIF/65448-54-6.gif)
65448-54-6
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22817-26-1
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$60.47/250mg
Yield:22817-26-1 89%
Reaction Conditions:
Stage #1: 2,3-dihydro-(2-phenylmethyl)-1H-benz[de]isoquinolinewith chloroformic acid ethyl ester in dichloromethane; for 8 h;Heating;
Stage #2: with potassium hydroxide;hydrazine in ethylene glycol; for 4 h;Heating;
References:
Zheng, Shijun;Lan, Jie;Khan, Saeed I.;Rubin, Yves [Journal of the American Chemical Society,2003,vol. 125,# 19,p. 5786 - 5791]
81-83-4
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22817-26-1
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$60.47/250mg
![1H-Benz[de]isoquinoline-1,3(2H)-dione,2-(phenylmethyl)-](/CAS/20180529/GIF/2896-24-4.gif)
2896-24-4
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22817-26-1
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![1H-Benz[de]isoquinolin-1-one, 2,3-dihydro-](/CAS/20200611/GIF/18833-41-5.gif)
81-84-5
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$13.00/25g
22817-26-1
45 suppliers
$60.47/250mg