2,2-DIMETHYL-5-VINYL-[1,3]DIOXOLANE-4-CARBALDEHYDE synthesis
- Product Name:2,2-DIMETHYL-5-VINYL-[1,3]DIOXOLANE-4-CARBALDEHYDE
- CAS Number:4105-60-6
- Molecular formula:C8H12O3
- Molecular Weight:156.18
114817-96-8
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4105-60-6
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Yield:4105-60-6 92%
Reaction Conditions:
Stage #1: [(4R,5R)-2,2-dimethyl-5-vinyl-1,3-dioxolan-4-yl]methanolwith sulfur trioxide pyridine complex;triethylamine in dichloromethane at -10; for 0.0833333 h;Inert atmosphere;
Stage #2: with dimethylsulfone in dichloromethane; for 0.25 h;Inert atmosphere;
References:
Sabitha, Gowravaram;Shankaraiah, Kontham;Yadav, Jhillu S. [European Journal of Organic Chemistry,2013,# 22,p. 4870 - 4878]
168109-89-5
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![1,3-Dioxolane-4-carboxaldehyde, 5-[[[(1,1-dimethylethyl)dimethylsilyl]oxy]methyl]-2,2-dimethyl-, (4S,5R)-](/CAS/20210111/GIF/125993-65-9.gif)
125993-65-9
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