[S-(R,R)]-1,3,4,5-Tetrahydro-3-[(1-phenylethyl)amino]-2H-1-benzazepin-2-one synthesis

2synthesis methods

Product Name:[S-(R*,R*)]-1,3,4,5-Tetrahydro-3-[(1-phenylethyl)amino]-2H-1-benzazepin-2-one
CAS Number:197658-50-7
Molecular formula:C18H20N2O
Molecular Weight:280.36

86499-96-9 Synthesis

Yield:-

Steps:

Multi-step reaction with 2 steps
1: 93 percent / Na₂CO₃, propylene glycol / 3.5 h / 130 °C
2: 88 percent / odorless mineral spirits / 16 h / 140 °C

References:

Shieh;Carlson;Zaunius [Journal of Organic Chemistry,1997,vol. 62,# 23,p. 8271 - 8272]

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