(3-BENZYLAMINO-1-METHYL-PROPYL)-CARBAMIC ACID TERT-BUTYL ESTER synthesis
- Product Name:(3-BENZYLAMINO-1-METHYL-PROPYL)-CARBAMIC ACID TERT-BUTYL ESTER
- CAS Number:176982-58-4
- Molecular formula:C16H26N2O2
- Molecular Weight:278.39
79069-13-9
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176982-58-4
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Yield:-
Steps:
Multi-step reaction with 5 steps
1: 86 percent / Et3N / CH2Cl2 / 2 h / 20 °C
2: 72 percent / dimethylsulfoxide / 15 h / 40 - 45 °C
3: 94 percent / H2; NH3 / Raney Ni / ethanol / 15 h / 20 °C / 4500.36 Torr
4: 98 percent / 3 Angstroem molecular sieves / diethyl ether / 20 h / 20 °C
5: 84 percent / NaBH4 / ethanol / 3 h / 10 °C
References:
Lebreton, Luc;Jost, Eric;Carboni, Bertrand;Annat, Jocelyne;Vaultier, Michel;Dutartre, Patrick;Renaut, Patrice [Journal of Medicinal Chemistry,1999,vol. 42,# 23,p. 4749 - 4763]
126301-16-4
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176982-58-4
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172695-22-6
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176982-57-3
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$60.00/50mg
176982-58-4
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