1-(((2R,4R)-4-((Benzyloxy)methyl)-2-(2,4-difluorophenyl)tetrahydrofuran-2-yl)methyl)-1H-1,2,4-triazole synthesis
- Product Name:1-(((2R,4R)-4-((Benzyloxy)methyl)-2-(2,4-difluorophenyl)tetrahydrofuran-2-yl)methyl)-1H-1,2,4-triazole
- CAS Number:165115-83-3
- Molecular formula:C21H21F2N3O2
- Molecular Weight:385.41
3587-60-8
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Yield:-
Steps:
Multi-step reaction with 4 steps
1: 1.) TiCl4; 2.) Et3N / 1.) CH2Cl2, 0 deg C
2: 85 percent / LAH / tetrahydrofuran / 0 °C
3: 96 percent / I2 / acetonitrile; pyridine / 0 - 5 °C
4: 81 percent / DMPU / dimethylformamide / 24 h / 100 °C
References:
Saksena, Anil K.;Girijavallabhan, Viyyoor M.;Wang, Haiyan;Liu, Yi-Tsung;Pike, Russell E.;Ganguly, Ashit K. [Tetrahedron Letters,1996,vol. 37,# 32,p. 5657 - 5660]
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