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ChemicalBook CAS DataBase List 1-(((2R,4R)-4-((Benzyloxy)methyl)-2-(2,4-difluorophenyl)tetrahydrofuran-2-yl)methyl)-1H-1,2,4-triazole
165115-83-3

1-(((2R,4R)-4-((Benzyloxy)methyl)-2-(2,4-difluorophenyl)tetrahydrofuran-2-yl)methyl)-1H-1,2,4-triazole synthesis

6synthesis methods
3587-60-8 Synthesis
Benzyl chloromethyl ether

3587-60-8
323 suppliers
$10.00/1g

1-(((2R,4R)-4-((Benzyloxy)methyl)-2-(2,4-difluorophenyl)tetrahydrofuran-2-yl)methyl)-1H-1,2,4-triazole

165115-83-3
20 suppliers
inquiry

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Yield:-

Steps:

Multi-step reaction with 4 steps
1: 1.) TiCl4; 2.) Et3N / 1.) CH2Cl2, 0 deg C
2: 85 percent / LAH / tetrahydrofuran / 0 °C
3: 96 percent / I2 / acetonitrile; pyridine / 0 - 5 °C
4: 81 percent / DMPU / dimethylformamide / 24 h / 100 °C

References:

Saksena, Anil K.;Girijavallabhan, Viyyoor M.;Wang, Haiyan;Liu, Yi-Tsung;Pike, Russell E.;Ganguly, Ashit K. [Tetrahedron Letters,1996,vol. 37,# 32,p. 5657 - 5660]

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