2,3,4,5-TETRAHYDRO-1H-BENZO[D]AZEPINE-7-CARBOXYLIC ACID HYDROCHLORIDE synthesis
- Product Name:2,3,4,5-TETRAHYDRO-1H-BENZO[D]AZEPINE-7-CARBOXYLIC ACID HYDROCHLORIDE
- CAS Number:149353-83-3
- Molecular formula:C11H14ClNO2
- Molecular Weight:0
10533-22-9
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149353-83-3
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Yield:-
Steps:
Multi-step reaction with 3 steps
1.1: aluminum (III) chloride / 1,1-dichloroethane / 2 h / 0 - 20 °C
1.2: 0 °C
2.1: sodium hydroxide; bromine / 1 h / 20 °C
3.1: hydrogenchloride; water / 120 h / Heating / reflux
References:
WO2008/135526,2008,A1
149353-98-0
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149353-83-3
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inquiry