benzaMide, N-(3,5-dichloro-4-pyridinyl)-4-(difluoroMethoxy)-3-hydroxy- synthesis
- Product Name:benzaMide, N-(3,5-dichloro-4-pyridinyl)-4-(difluoroMethoxy)-3-hydroxy-
- CAS Number:1391052-76-8
- Molecular formula:C13H8Cl2F2N2O3
- Molecular Weight:349.12
151103-08-1
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$8.00/250mg
1391052-76-8
72 suppliers
$132.00/1mg
Yield:-
Steps:
Multi-step reaction with 3 steps
1.1: aminosulfonic acid; sodium chlorite / acetonitrile; water / 0 - 30 °C
2.1: N,N-dimethyl-formamide; thionyl chloride / toluene / 3 h / 90 °C / Reflux
3.1: sodium hydride / acetonitrile / 2 h / 0 - 5 °C
3.2: 1.5 h / 0 - 15 °C
References:
Lin, Yan;Huang, Peijun;Qi, Haofei;Chen, Ligong;Wang, Donghua [Research on Chemical Intermediates,2013,vol. 39,# 7,p. 3111 - 3115]
22889-78-7
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$6.00/5g
1401228-67-8
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1391052-76-8
72 suppliers
$132.00/1mg
4837-20-1
139 suppliers
$40.00/5g
1391052-76-8
72 suppliers
$132.00/1mg
57320-63-5
38 suppliers
$63.00/1g
1391052-76-8
72 suppliers
$132.00/1mg