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ChemicalBook CAS DataBase List 4-METHOXYPHENYL 3-O-BENZYL-2-DEOXY-2-PHTHALIMIDO-BETA-D-GLUCOPYRANOSIDE
138906-44-2

4-METHOXYPHENYL 3-O-BENZYL-2-DEOXY-2-PHTHALIMIDO-BETA-D-GLUCOPYRANOSIDE synthesis

4synthesis methods
10022-13-6 Synthesis
1,3,4,6-TETRA-O-ACETYL-2-DEOXY-2-PHTHALIMIDO-BETA-D-GLUCOPYRANOSE

10022-13-6
104 suppliers
$14.00/1G

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Yield:-

Steps:

Multi-step reaction with 4 steps
1: 84 percent / Me3SiOTf / 1,2-dichloro-ethane / 3 h / 0 °C
2: p-TsOH*H2O / dimethylformamide / 20 h / 20 °C
3: 61 percent / NaH / dimethylformamide / 20 h / 20 °C
4: 77 percent / p-TsOH*H2O / methanol; dioxane / 1) 1 h, 60 deg C, 2) 45 min, 85 deg C

References:

Nakano;Ito;Ogawa [Carbohydrate Research,1993,vol. 243,# 1,p. 43 - 69]

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