N-[1-Deoxy-3,4:5,6-bis-O-(1-methylethylidene)-D-glucitol-1-yl]-N2-[(9H-fluoren-9-ylmethoxy)carbonyl]-L-glutamine 2-propen-1-yl ester synthesis
- Product Name:N-[1-Deoxy-3,4:5,6-bis-O-(1-methylethylidene)-D-glucitol-1-yl]-N2-[(9H-fluoren-9-ylmethoxy)carbonyl]-L-glutamine 2-propen-1-yl ester
- CAS Number:1227510-36-2
- Molecular formula:C35H44N2O10
- Molecular Weight:652.73
144120-54-7
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Yield:1227510-36-2 50%
Reaction Conditions:
with benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate;N-ethyl-N,N-diisopropylamine in N,N-dimethyl-formamide at 20; for 2 h;Inert atmosphere;
References:
Vlahov, Iontcho R.;Santhapuram, Hari Krishna R.;You, Fei;Wang, Yu;Kleindl, Paul J.;Hahn, Spencer J.;Vaughn, Jeremy F.;Reno, Daniel S.;Leamon, Christopher P. [Journal of Organic Chemistry,2010,vol. 75,# 11,p. 3685 - 3691] Location in patent:experimental part