4-(6-Amino-pyridin-2-yl)-piperazine-1-carboxylic acid tert-butyl ester synthesis
- Product Name:4-(6-Amino-pyridin-2-yl)-piperazine-1-carboxylic acid tert-butyl ester
- CAS Number:1206248-85-2
- Molecular formula:C14H22N4O2
- Molecular Weight:278.35
19798-81-3
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Yield:1206248-85-2 45%
Reaction Conditions:
with {Ni(2,2'-bipyridine)3}Br2;tetrabutylammomium bromide;1,8-diazabicyclo[5.4.0]undec-7-ene in N,N-dimethyl acetamide at 20; for 4 h;Electrolysis;Inert atmosphere;
References:
Kawamata, Yu;Vantourout, Julien C.;Hickey, David P.;Bai, Peng;Chen, Longrui;Hou, Qinglong;Qiao, Wenhua;Barman, Koushik;Edwards, Martin A.;Garrido-Castro, Alberto F.;Degruyter, Justine N.;Nakamura, Hugh;Knouse, Kyle;Qin, Chuanguang;Clay, Khalyd J.;Bao, Denghui;Li, Chao;Starr, Jeremy T.;Garcia-Irizarry, Carmen;Sach, Neal;White, Henry S.;Neurock, Matthew;Minteer, Shelley D.;Baran, Phil S. [Journal of the American Chemical Society,2019,vol. 141,# 15,p. 6392 - 6402] Location in patent:supporting information