5-[(1,3-DIOXO-1,3-DIHYDRO-2H-ISOINDOL-2-YL)METHYL]-2-FURALDEHYDE synthesis
- Product Name:5-[(1,3-DIOXO-1,3-DIHYDRO-2H-ISOINDOL-2-YL)METHYL]-2-FURALDEHYDE
- CAS Number:116750-06-2
- Molecular formula:C14H9NO4
- Molecular Weight:255.23
1623-88-7
87 suppliers
$60.00/25mg
1074-82-4
482 suppliers
$5.00/25g
116750-06-2
29 suppliers
$57.00/250mg
Yield:116750-06-2 89.5%
Reaction Conditions:
in N,N-dimethyl-formamide at 80; for 3 h;Gabriel Amine Synthesis;Temperature;
Steps:
1.1; 2.1; 3.1; 4.1 (1) Gabriel reaction
Put 102mg of 5-CMF, 185mg of KPI, and 20mL of DMF in a round-bottomed flask and mix well. At 80 ° C, react for 3 hours. After the reaction, filter and collect the filtrate. Add 4 ° C deionized water to the filtrate and let stand. After 30 min, filtering and collecting solids, the 5-PMF yield was determined to be 89.5%.
References:
CN110330440,2019,A Location in patent:Paragraph 0025; 0027-0028; 0036-0038; 0045-0047; 0054-0056
617-89-0
272 suppliers
$16.00/25g
116750-06-2
29 suppliers
$57.00/250mg
85-44-9
763 suppliers
$9.00/5g
116750-06-2
29 suppliers
$57.00/250mg