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23373-78-6

1-TERT-BUTYL-1H-PYRROLE-2-CARBALDEHYDE synthesis

6synthesis methods
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Yield:23373-78-6 4 %Spectr. ,30186-46-0 96 %Spectr.

Reaction Conditions:

Stage #1: 1-(t-butyl)pyrrole;N,N-diisorpopylformamidewith trichlorophosphate in 1,1-dichloroethane; for 1 h;Reflux;Vilsmeier-Haack reaction;
Stage #2: with potassium hydroxide in 1,1-dichloroethane;water; for 0.0166667 h;

References:

Ilyin, Petrv.;Pankova, Alenas.;Kuznetsov, Mikhail A. [Synthesis,2012,vol. 44,# 9,p. 1353 - 1358] Location in patent:experimental part

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