1-TERT-BUTYL-1H-PYRROLE-2-CARBALDEHYDE synthesis
- Product Name:1-TERT-BUTYL-1H-PYRROLE-2-CARBALDEHYDE
- CAS Number:23373-78-6
- Molecular formula:C9H13NO
- Molecular Weight:151.21
24764-40-7
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2700-30-3
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23373-78-6
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30186-46-0
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Yield:23373-78-6 4 %Spectr. ,30186-46-0 96 %Spectr.
Reaction Conditions:
Stage #1: 1-(t-butyl)pyrrole;N,N-diisorpopylformamidewith trichlorophosphate in 1,1-dichloroethane; for 1 h;Reflux;Vilsmeier-Haack reaction;
Stage #2: with potassium hydroxide in 1,1-dichloroethane;water; for 0.0166667 h;
References:
Ilyin, Petrv.;Pankova, Alenas.;Kuznetsov, Mikhail A. [Synthesis,2012,vol. 44,# 9,p. 1353 - 1358] Location in patent:experimental part
1003-29-8
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507-20-0
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23373-78-6
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24764-40-7
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4497-57-8
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23373-78-6
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30186-46-0
15 suppliers
$65.00/50mg
24764-40-7
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607-00-1
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23373-78-6
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$45.00/10mg
30186-46-0
15 suppliers
$65.00/50mg
24764-40-7
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52008-97-6
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23373-78-6
9 suppliers
$45.00/10mg
30186-46-0
15 suppliers
$65.00/50mg