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120964-49-0

1-O-HEXADECYL-2-O-METHYL-SN-GLYCEROL synthesis

6synthesis methods
36653-82-4 Synthesis
1-Hexadecanol

36653-82-4
529 suppliers
$6.00/100g

1-O-HEXADECYL-2-O-METHYL-SN-GLYCEROL

120964-49-0
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Yield:-

Steps:

Multi-step reaction with 3 steps
1: 79 percent / BF3 etherate / CHCl3 / 24 h
2: 89 percent / 2,6-di-tert-butyl-4-methylpyridine / CH2Cl2 / 16 h / Heating
3: 89 percent / potassium superoxide / 18-crown-6 / dimethylsulfoxide; dimethylformamide; 1,2-dimethoxy-ethane / 6 h / Ambient temperature

References:

Guivisdalsky, Pedro N.;Bittman, Robert [Journal of Organic Chemistry,1989,vol. 54,# 19,p. 4637 - 4642]

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