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ChemicalBook CAS DataBase List 1-Nonaneboronic acid
3088-78-6

1-Nonaneboronic acid synthesis

6synthesis methods
1,3,2-Dioxaborolane, 4,4,5,5-tetramethyl-2-(4-nonylphenyl)-

1356840-19-1
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Yield:-

Steps:

Multi-step reaction with 4 steps
1: dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; potassium phosphate monohydrate; palladium diacetate / toluene
2: palladium on activated charcoal; hydrogen / ethanol
3: hydrogenchloride; sodium nitrite / water / Cooling with ice
4: dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; palladium diacetate; triethylamine / 1,4-dioxane / 80 °C

References:

O'Connell, Daniel P.;Leblanc, Daniel F.;Cromley, Debra;Billheimer, Jeffrey;Rader, Daniel J.;Bachovchin, William W. [Bioorganic and Medicinal Chemistry Letters,2012,vol. 22,# 3,p. 1397 - 1401]

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