1-methylene-1,2,3,4-tetrahydronaphthalene synthesis
9synthesis methods
- Product Name:1-methylene-1,2,3,4-tetrahydronaphthalene
- CAS Number:25108-63-8
- Molecular formula:C11H12
- Molecular Weight:144.21
Yield:25108-63-8 100%
Reaction Conditions:
with n-butyllithium in tetrahydrofuran;hexane;Inert atmosphere;Cooling with ice;Wittig reaction;
References:
Larsen, Casey R.;Grotjahn, Douglas B. [Journal of the American Chemical Society,2012,vol. 134,# 25,p. 10357 - 10360] Location in patent:supporting information; experimental part