1-METHYL-2-TRIFLUOROMETHYLSULFANYL-BENZENE synthesis
- Product Name:1-METHYL-2-TRIFLUOROMETHYLSULFANYL-BENZENE
- CAS Number:1736-75-0
- Molecular formula:C8H7F3S
- Molecular Weight:192.2
Yield:1736-75-0 92 %Spectr.
Reaction Conditions:
Stage #1: 2-methylphenyl diazonium tetrafluoroboratewith copper(I) thiocyanate;sodium thiocyanide;caesium carbonate in acetonitrile at 20; for 0.166667 h;Inert atmosphere;
Stage #2: (trifluoromethyl)trimethylsilane in acetonitrile at 20; for 16 h;Inert atmosphere;
References:
Danoun, Gregory;Bayarmagnai, Bilguun;Gruenberg, Matthias F.;Goossen, Lukas J. [Chemical Science,2014,vol. 5,# 4,p. 1312 - 1316]
16419-60-6
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2923-18-4
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1736-75-0
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615-37-2
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3872-23-9
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1736-75-0
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2093-46-1
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3872-23-9
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1736-75-0
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1736-75-0
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