1-Hydroxy-2-naphthoic acid synthesis
- Product Name:1-Hydroxy-2-naphthoic acid
- CAS Number:86-48-6
- Molecular formula:C11H8O3
- Molecular Weight:188.18
90-15-3
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86-48-6
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Yield:-
Steps:
Multi-step reaction with 4 steps
1.1: 1H-imidazole / N,N-dimethyl-formamide / 0.5 h / 0 - 20 °C / Inert atmosphere
1.2: 0 - 20 °C / Inert atmosphere
2.1: water; sodium hydrogencarbonate / N,N-dimethyl-formamide; diethyl ether / 0.5 h / 20 °C / Inert atmosphere
3.1: palladium diacetate; silver(I) acetate; N-tert-butoxycarbonyl-L-leucine; 2,2,2-trifluoroethanol / 1,2-dichloro-ethane / 0.08 h / 95 °C / Inert atmosphere
3.2: 18 h / 95 °C / Inert atmosphere
4.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 0.5 h / Inert atmosphere
References:
Wang, Yang;Gevorgyan, Vladimir [Angewandte Chemie - International Edition,2015,vol. 54,# 7,p. 2255 - 2259][Angew. Chem.,2015,vol. 127,# 7,p. 2283 - 2287,5]
90-15-3
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86-48-6
326 suppliers
$5.00/25g
