1-DODECYL-3-PHENYL-2-THIOUREA synthesis
1synthesis methods
- Product Name:1-DODECYL-3-PHENYL-2-THIOUREA
- CAS Number:63980-78-9
- Molecular formula:C19H32N2S
- Molecular Weight:320.54
Yield:63980-78-9 98%
Reaction Conditions:
in toluene;
Steps:
2.1.1 Example 2.1.1. Thiourea synthesis: N-phenyl-N'-dodecylthiourea (3d):
N- dodecyl-N'-phenylthiourea was prepared according to the general procedure from solutions of n- dodecylamine (1 1 .56 g, 62.4 mmol) in toluene (20 mL) and phenyl isothiocyanate (8.44 g, 62.4 mmol) in toluene (20 mL), producing a white powder. Yield: 19.56 g (98%).
References:
WO2016/115416,2016,A1 Location in patent:Paragraph 0204; 0205