1-cyano-2-hydroxy-3-butene synthesis
- Product Name:1-cyano-2-hydroxy-3-butene
- CAS Number:27451-36-1
- Molecular formula:C5H7NO
- Molecular Weight:97.12
Yield:27451-36-1 92%
Reaction Conditions:
with n-butyllithium;diisopropylamine in tetrahydrofuran;hexane1.) 10 deg C, 1 h; -78 deg C, 1 h, 2.) -78 deg C, 3 h;
References:
Itoh, Toshiyuki;Mitsukura, Koichi;Kanphai, Wipa;Takagi, Yumiko;Kihara, Hiroshi;Tsukube, Hiroshi [Journal of Organic Chemistry,1997,vol. 62,# 26,p. 9165 - 9172]
87487-95-4
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