1-BUTANOL-4,4,4-D3 synthesis
- Product Name:1-BUTANOL-4,4,4-D3
- CAS Number:64156-70-3
- Molecular formula:C4H10O
- Molecular Weight:74.12
![2-Butan-1,1,1-d3-ol, 4-[[(1,1-dimethylethyl)dimethylsilyl]oxy]-, 2-(4-methylbenzenesulfonate)](/CAS/20211123/GIF/1337571-69-3.gif)
1337571-69-3
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64156-70-3
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$903.50/500MG
Yield:64156-70-3 60%
Reaction Conditions:
Stage #1: (+/-)-[1,1,1-d3]-4-(tert-butyldimethylsilyloxy)-2-(p-toluenesulfonyloxy)butanewith lithium aluminium deuteride in diethyl ether; for 4 h;Inert atmosphere;Reflux;
Stage #2: with hydrogenchloride;water in diethyl ether;Inert atmosphere;
References:
Khrizman, Alexander;Cheng, Hiu Yan;Moyna, Guillermo [Journal of labelled compounds and radiopharmaceuticals,2011,vol. 54,# 8,p. 401 - 407] Location in patent:experimental part
36789-14-7
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64156-70-3
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$903.50/500MG
75-21-8
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7439-86-3
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64156-70-3
15 suppliers
$903.50/500MG