1-(bromomethyl)-2-chloro-4-nitrobenzene synthesis
- Product Name:1-(bromomethyl)-2-chloro-4-nitrobenzene
- CAS Number:42533-63-1
- Molecular formula:C7H5BrClNO2
- Molecular Weight:250.48
Yield:42533-63-1 248 mg
Reaction Conditions:
with N-Bromosuccinimide;dibenzoyl peroxide in tetrachloromethane at 80;
Steps:
18.1
Add 2-chloro-4-nitrotoluene (200mg, 1 equivalent), benzoyl peroxide (28mg, 0.1 equivalent), and N-bromosuccinimide (228mg, 1.1 equivalent) to 20ml of tetrachloride In carbonization, react overnight at 80°C in an oil bath. After the reaction was completed, the solvent was removed, and the crude product was subjected to column chromatography to obtain 248 mg of product.
References:
CN112010789,2020,A Location in patent:Paragraph 0102-0106
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