1-BROMO-4-CHLOROISOQUINOLINE synthesis
- Product Name:1-BROMO-4-CHLOROISOQUINOLINE
- CAS Number:925890-48-8
- Molecular formula:C9H5BrClN
- Molecular Weight:242.5
1532-91-8
83 suppliers
$41.00/1g
925890-48-8
32 suppliers
$100.00/100mg
Yield:-
Steps:
Multi-step reaction with 2 steps
1.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 14 h / 0 - 20 °C
2.1: tetrabutylammomium bromide / dichloromethane / 0.17 h / 20 °C / Inert atmosphere; Molecular sieve
2.2: 20 °C / Inert atmosphere
References:
Wengryniuk, Sarah E.;Weickgenannt, Andreas;Reiher, Christopher;Strotman, Neil A.;Chen, Ke;Eastgate, Martin D.;Baran, Phil S. [Organic Letters,2013,vol. 15,# 4,p. 792 - 795]