1-BOC-4-CARBOXYINDOLE synthesis
- Product Name:1-BOC-4-CARBOXYINDOLE
- CAS Number:848444-79-1
- Molecular formula:C14H15NO4
- Molecular Weight:261.27
124-38-9
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$214.00/14L
![1H-Indole-1-carboxylic acid, 4-[[(trifluoromethyl)sulfonyl]oxy]-, 1,1-dimethylethyl ester](/CAS/20210305/GIF/1195931-67-9.gif)
1195931-67-9
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848444-79-1
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$230.00/250mg
Yield:848444-79-1 65%
Reaction Conditions:
with (4,4'-di-tert-butyl-2,2'-dipyridyl)-bis-(2-phenylpyridine(-1H))-iridium(III) hexafluorophosphate;palladium diacetate;caesium carbonate;N-ethyl-N,N-diisopropylamine;DavePhos in N,N-dimethyl acetamide at 20; for 36 h;Irradiation;Green chemistry;chemoselective reaction;
References:
Bhunia, Samir Kumar;Das, Pritha;Nandi, Shantanu;Jana, Ranjan [Organic Letters,2019,vol. 21,# 12,p. 4632 - 4637] Location in patent:supporting information