1-AMINO-3-DIETHYLAMINO-2-PROPANOL synthesis
- Product Name:1-AMINO-3-DIETHYLAMINO-2-PROPANOL
- CAS Number:6322-01-6
- Molecular formula:C7H18N2O
- Molecular Weight:146.23
2917-91-1
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6322-01-6
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$171.00/1g
Yield:6322-01-6 92%
Reaction Conditions:
with ammonium hydroxide
Steps:
2.3 Step 3
Step 3 To the ice-cold solution of ammonium hydroxide (25 mL, 159 mmole) of 25% (w/w) was added glycidyldiethylamine dropwise (3.2 g, 24.8 mmol) over 10 minutes. The reaction mixture was stirred at 0-5° C. for 1 hour and then room temperature for 14 hours. The resulting reaction mixture was evaporated and distilled (84-90° C. at 500-600 mT) to yield 1-amino-3-diethylamino-propan-2-ol (3.3 g, 92%). MS m/z 147 ([M+1]+·).
References:
US2003/92917,2003,A1
15285-59-3
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6322-01-6
17 suppliers
$171.00/1g
2917-91-1
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7664-41-7
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$15.00/100ml
6322-01-6
17 suppliers
$171.00/1g