1-(6-AMino-2,3-diMethoxy-phenyl)-ethanone synthesis
- Product Name:1-(6-AMino-2,3-diMethoxy-phenyl)-ethanone
- CAS Number:98300-41-5
- Molecular formula:C10H13NO3
- Molecular Weight:195.2151
98300-40-4
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98300-41-5
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Yield:98300-41-5 95%
Reaction Conditions:
palladium-carbon in methanol;
Steps:
17.A 6'-(N-2-Carbethoxyethylamino)-2',3'-dimethoxyacetophenone
Catalytic hydrogenation of 2,3-dimethoxy-6-nitroacetophenone in MeOH with 10% Pd/C in a Parr apparatus afforded 6'-amino-2',3'-dimethoxyacetophenone (95% yield), mp 57°-58° C.
References:
US4556739,1985,A
72517-26-1
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