1-(4-BROMO-2-FLUOROPHENYL)HYDRAZINE HYDROCHLORIDE synthesis
- Product Name:1-(4-BROMO-2-FLUOROPHENYL)HYDRAZINE HYDROCHLORIDE
- CAS Number:299440-17-8
- Molecular formula:C6H6BrFN2
- Molecular Weight:205.03
367-24-8
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Yield:299440-17-8 76.2%
Reaction Conditions:
Stage #1: 4-bromo-2-fluoroanilinewith hydrogenchloride;sodium nitrite in water at 0 - 5; for 0.166667 h;
Stage #2: with hydrogenchloride;tin(ll) chloride in water;cooling;
References:
Makhija, Mahindra T.;Kasliwal, Rajesh T.;Kulkarni, Vithal M.;Neamati, Nouri [Bioorganic and Medicinal Chemistry,2004,vol. 12,# 9,p. 2317 - 2333]