1,4-Benzenedicarbonyl dichloride, 2,5-dibromo- synthesis
- Product Name:1,4-Benzenedicarbonyl dichloride, 2,5-dibromo-
- CAS Number:13815-90-2
- Molecular formula:C8H2Br2Cl2O2
- Molecular Weight:360.81
106-42-3
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Yield:-
Steps:
Multi-step reaction with 3 steps
1.1: iodine / dichloromethane / 1 h / 0 °C
1.2: 16 h / 0 - 20 °C / Darkness
2.1: pyridine / Reflux
2.2: Reflux
2.3: 90 °C
3.1: thionyl chloride / toluene; N,N-dimethyl-formamide / 2 h / Reflux
References:
Rodrigues, Ana Clara B.;Wetterling, Dario;Scherf, Ullrich;Seixas de Melo, J. Sérgio [Chemistry - A European Journal,2021,vol. 27,# 29,p. 7826 - 7830]
13731-82-3
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1074-24-4
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97935-32-5
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