ChemicalBook CAS DataBase List 1,4,7,10,13,16-HEXAAZACYCLOOCTADECANE

1,4,7,10,13,16-HEXAAZACYCLOOCTADECANE synthesis

5synthesis methods

Product Name:1,4,7,10,13,16-HEXAAZACYCLOOCTADECANE
CAS Number:296-35-5
Molecular formula:C12H30N6
Molecular Weight:258.41

4439-20-7 Synthesis

4439-20-7
184 suppliers
$8.00/5g

296-35-5
67 suppliers
$143.00/250 mg

Yield:-

Steps:

Multi-step reaction with 3 steps
1: 72 percent / 30percent NaOH / triethylbenzylammonium chloride / H₂O; CH₂Cl₂ / 10 - 15 °C
2: 85 percent / 5percent NaOH / tetrabutylammonium iodide / H₂O; toluene / Heating; 8-10 h
3: 75 percent / conc. H₂SO₄ / 100 - 105 °C / Heating; 50-70 h

References:

Luk'yanenko, N. G.;Basok, S. S.;Filonova, L. K.;Kulikov, N. V.;Pastushok, V. N. [Chemistry of Heterocyclic Compounds,1990,vol. 26,# 3,p. 346 - 349][Khimiya Geterotsiklicheskikh Soedinenii,1990,# 3,p. 401 - 404]

56187-09-8 Synthesis