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1,3-Propanediol, 2-amino-1-phenyl-, (1R,2S)- synthesis

3synthesis methods

Product Name:1,3-Propanediol, 2-amino-1-phenyl-, (1R,2S)-
CAS Number:105452-39-9
Molecular formula:C9H13NO2
Molecular Weight:167.21

Benzenepropanoic acid, α,β-dihydroxy-, ethyl ester, (αS,βR)-

108741-12-4
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1,3-Propanediol, 2-amino-1-phenyl-, (1R,2S)-

105452-39-9
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Yield:-

Steps:

Multi-step reaction with 3 steps
1: triethylamine / dichloromethane
2: sodium azide / N,N-dimethyl-formamide
3: lithium borohydride / tetrahydrofuran

References:

Liu, Zhuqing;Shultz, C.Scott;Sherwood, Candice A.;Krska, Shane;Dormer, Peter G.;Desmond, Richard;Lee, Claire;Sherer, Edward C.;Shpungin, Joseph;Cuff, James;Xu, Feng [Tetrahedron Letters,2011,vol. 52,# 14,p. 1685 - 1688]

ethyl-(E)-cinnamate,ethyl-trans-cinnamate

4192-77-2
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$11.00/25g

105452-39-9
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References

Acetamide, N-[2-hydroxy-1-(hydroxymethyl)-2-phenylethyl]-

91247-54-0
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28143-91-1 Synthesis

(1S,2S)-(+)-2-Amino-1-phenyl-1,3-propanediol

28143-91-1
164 suppliers
$41.78/1g

(1R,2R)-(-)-2-Amino-1-phenyl-1,3-propanediol

46032-98-8
143 suppliers
$45.00/50mg

105452-39-9
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1,3-Propanediol, 2-amino-1-phenyl-, (1S,2R)-

119364-52-2
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References

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1,3-Propanediol, 2-amino-1-phenyl-, (1R,2S)- synthesis