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ChemicalBook CAS DataBase List 1,2:5,6-Di-O-isopropylidene-alpha-D-allofuranose
2595-05-3

1,2:5,6-Di-O-isopropylidene-alpha-D-allofuranose synthesis

10synthesis methods
-

Yield:-

Steps:

Multi-step reaction with 3 steps
1: 68 percent / ZnCl2; aq. H3PO4 / 36 h / 20 °C
2: 91 percent / pyridinium dichromate; acetic anhydride / CH2Cl2 / 4 h / 75 °C
3: 90 percent / NaBH4 / ethanol; H2O / 1 h / 0 °C

References:

Guo, Jiantao;Frost [Journal of the American Chemical Society,2002,vol. 124,# 36,p. 10642 - 10643]

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