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ChemicalBook CAS DataBase List 1,2,3-TRICHLOROPROPENE

1,2,3-TRICHLOROPROPENE synthesis

7synthesis methods

Product Name:1,2,3-TRICHLOROPROPENE
CAS Number:96-19-5
Molecular formula:C3H3Cl3
Molecular Weight:145.41

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Yield:-

Reaction Conditions:

with chlorine at 60 - 80;

Steps:

1
8gr of chlorine gas and methylacetylene gas at molar ratio of 4/1 chlorine to methylacetylene is sparged for 30 minutes in a 100 ml mixture of 50/50 mole% of 1, 1 ,2,2- tetrachloropropane and 1,2,2,3-tetrachloropropane as a solvent heated in a water bath and stirred to maintain the temperature at 60-80°C. A reflux column is placed to return solvent, unreacted chlorine and product. The product of the reaction is expected to contain 15 mole% 1,2,3-trichloropropene, 20 mole% 1,2,2,3-tetrachloropropane, and 65 moie% 1, 1,2,2- tetrachloropropane

References:

DOW GLOBAL TECHNOLOGIES, LLC;TIRTOWIDJOJO, Max Markus;FISH, Barry;KRUPER, William J. WO2013/74394, 2013, A1 Location in patent:Paragraph 0078

13116-53-5
78 suppliers
$35.00/1 g

96-19-5
86 suppliers
$14.00/1g

References