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ChemicalBook CAS DataBase List 1,1-DIETHYLUREA
634-95-7

1,1-DIETHYLUREA synthesis

10synthesis methods
-

Yield: 30%

Reaction Conditions:

in hexane

Steps:

9 EXAMPLE 9
EXAMPLE 9 As described in Example 4, but using 365.3 g of diethylamine (5.0 mol) and using n-hexane as the diluent, diethylurea having a melting point of 68 -70° C. was obtained in a yield of 30% of theory after recrystallizing from diisopropyl ether.

References:

Chemie Linz Gesellschaft m.b.H. US5043444, 1991, A

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