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ChemicalBook CAS DataBase List 1,1-DIBROMOPINACOLONE
30263-65-1

1,1-DIBROMOPINACOLONE synthesis

12synthesis methods
-

Yield:-

Steps:

Multi-step reaction with 2 steps
1.1: dichloromethane; tetrahydrofuran / 20 °C / Cooling with ice
2.1: toluene / 65 °C / Schlenk technique; Inert atmosphere
2.2: -78 °C / Schlenk technique; Inert atmosphere
2.3: 1 h / 20 °C / Schlenk technique; Inert atmosphere

References:

Kobeissi, Marwan;Cherry, Khalil;Jomaa, Wissam [Synthetic Communications,2013,vol. 43,# 21,p. 2955 - 2965]

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