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ChemicalBook CAS DataBase List 1,1,3,3,5,5-HEXAMETHYLTRISILOXANE
1189-93-1

1,1,3,3,5,5-HEXAMETHYLTRISILOXANE synthesis

14synthesis methods
-

Yield:1189-93-1 82%

Reaction Conditions:

in water at 20; for 72 h;

Steps:



TMDS, dimethyldichlorosilane, and deionized water were added, and the solution was mixed for three days at room temperature. Then, the crude product was neutralized, dried, and distilled under reduced pressure. A colorless transparent liquid was obtained and denoted as TTDS. Yield: about 82%. As shown in Scheme 1. 1H NMR (600MHz, Chloroform-d) δ 4.71 (m, 1H), 0.21 (m, 6H), 0.09 (m, 3H).

References:

Luo, Shuai;Dai, Xueyan;Sui, Yanlong;Li, Peihong;Zhang, Chunling [Polymer,2021,vol. 218,art. no. 123522]

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