N,N-二乙基環(huán)己胺(91-65-6)紅外圖譜(IR2)
InChI:InChI=1S/C10H21N/c1-3-11(4-2)10-8-6-5-7-9-10/h10H,3-9H2,1-2H3
InChIKey: CIXSDMKDSYXUMJ-UHFFFAOYSA-N
Smiles:C1(N(CC)CC)CCCCC1
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Mass
MS-NW-0890
N,N-diethylcyclohexylamine
C10H21N (Mass of molecular ion: 155)
Source Temperature: 270 °C
Sample Temperature: 150 °C
Reservoir, 75 eV
27.0 7.7
28.0 14.0
29.0 12.5
30.0 5.5
39.0 5.0
41.0 14.9
42.0 7.4
43.0 2.3
44.0 6.0
53.0 2.5
54.0 3.4
55.0 12.4
56.0 18.9
57.0 1.7
58.0 29.0
67.0 1.7
68.0 1.6
69.0 1.4
70.0 5.9
71.0 11.3
72.0 6.0
81.0 1.4
82.0 2.0
83.0 3.4
84.0 14.6
85.0 1.3
86.0 3.6
96.0 1.4
98.0 5.8
99.0 6.4
110.0 1.4
112.0 100.0
113.0 8.6
126.0 3.3
140.0 13.5
141.0 1.3
154.0 1.8
155.0 15.6
156.0 1.8
400 MHz in CDCl3
90 MHz in CDCl3
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| 1H NMR |
399.65 MHz |
| C10 H21 N
|
0.05 ml : 0.5 ml CDCl3
|
| N,N-diethylcyclohexylamine
|
 |
Assign. Shift(ppm)
A 2.540
B 2.48
C 1.79
D 1.620
E 1.21
F 1.10
G 1.026
|
Hz ppm Int.
1026.12 2.568 219
1018.92 2.550 580
1011.72 2.532 590
1004.52 2.514 238
992.19 2.483 56
722.29 1.808 110
712.16 1.782 130
653.93 1.637 46
641.60 1.606 49
498.66 1.248 60
488.28 1.222 148
486.45 1.218 157
482.79 1.209 65
478.52 1.198 173
477.66 1.196 168
469.60 1.176 67
468.75 1.173 64
467.77 1.171 64
417.24 1.045 628
410.03 1.026 1000
402.83 1.008 599
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| 1H NMR |
89.56 MHz |
| C10 H21 N
|
0.04 ml : 0.5 ml CDCl3
|
| N,N-diethylcyclohexylamine
|
|
Assign. Shift(ppm)
A 2.532
B 2.53
C 1.78
D 1.18
E 1.03
|
Hz ppm Int.
238.75 2.666 101
235.19 2.627 23
231.25 2.583 406
228.81 2.555 29
224.13 2.503 455
219.69 2.453 23
217.31 2.427 152
157.06 1.754 116
105.31 1.176 117
98.63 1.102 519
91.69 1.024 1000
84.38 0.943 359