701-70-2

乙基苯乙醇(701-70-2)質(zhì)譜(MS)

產(chǎn)品名稱:乙基苯乙醇

CAS:701-70-2

分子式:C10H14O

分子量: 150.22

Mass

MS-NW-7333          
(-)-alpha-ethylphenethyl alcohol
C10H14O             (Mass of molecular ion:    150)

   Source Temperature: 210 °C
   Sample Temperature: 190 °C
   Reservoir, 75 eV

      27.0       1.6
      29.0       1.9
      31.0       7.9
      39.0       3.4
      41.0       4.9
      43.0       1.0
      50.0       1.0
      51.0       3.1
      57.0       2.0
      59.0      19.5
      63.0       1.9
      65.0       6.7
      77.0       4.0
      78.0       1.4
      79.0       1.4
      89.0       1.5
      91.0      40.8
      92.0     100.0
      93.0       8.5
     103.0       5.8
     121.0       5.9

90 MHz in CDCl3

¹H NMR	89.56 MHz
C₁₀ H₁₄ O	0.05 ml : 0.5 ml CDCl₃
(-)-alpha-ethylphenethyl alcohol

    Assign.     Shift(ppm)

      A          7.23 to 7.21
      B             3.693
      C     *1      2.77
      D     *1      2.62
      E             1.92
      F             1.49
      G             0.97
     
     J(B,C)=4.7HZ
     J(B,D)=8.0HZ

     Hz     ppm     Int.

    663.00   7.403     32
    659.69   7.366     43
    657.00   7.336     63
    654.69   7.311     76
    651.88   7.279    193
    651.13   7.271    183
    650.19   7.260    189
    647.63   7.232   1000
    646.19   7.216    903
    643.38   7.184    227
    641.38   7.162    144
    640.75   7.155    148
    638.56   7.130    103
    635.63   7.098     44
    633.75   7.077     38
    632.81   7.066     34
    338.13   3.776     55
    336.94   3.763     49
    336.75   3.761     49
    335.44   3.746     50
    332.81   3.717     55
    330.69   3.693     78
    328.94   3.673     57
    326.31   3.644     51
    325.31   3.633     57
    325.00   3.629     57
    323.94   3.618     66
    318.63   3.558     35
    260.75   2.912     38
    255.88   2.858     46
    247.19   2.761    226
    242.44   2.708    427
    238.31   2.661     36
    237.81   2.656     35
    237.38   2.651     36
    236.88   2.645     37
    234.56   2.620    204
    228.94   2.557     51
    221.13   2.470     49
    171.75   1.918    206
    150.38   1.680     38
    148.31   1.656     38
    148.06   1.654     38
    145.00   1.620     42
    143.88   1.607     56
    142.00   1.586    134
    140.94   1.574    111
    138.69   1.549     57
    136.50   1.525    129
    134.13   1.498    281
    131.25   1.466     69
    128.63   1.437    166
    127.31   1.422    195
    124.06   1.386     32
    123.75   1.382     32
    121.38   1.356    106
    112.88   1.261     32
     93.06   1.040    374
     86.31   0.964    634
     78.56   0.878    199
     77.13   0.862    123

in CDCl3