65473-13-4

N-甲基-1-萘甲胺鹽酸鹽(65473-13-4)質(zhì)譜(MS)

產(chǎn)品名稱:N-甲基-1-萘甲胺鹽酸鹽

CAS:65473-13-4

分子式:C12H14ClN

分子量: 207.7

Mass

MS2015-05293CW      
N-methyl-1-naphthalenemethylamine hydrochloride
C12H13N HCl         (Mass of molecular ion:    171)

   Source Temperature: 245 °C
   Sample Temperature:  20 °C
   Direct, 70 eV

      28.0       1.8
      36.0       7.3
      38.0       2.4
      39.0       1.0
      42.0      16.7
      43.0       2.4
      44.0      16.8
      50.0       1.0
      51.0       1.8
      57.5       1.2
      62.0       1.0
      63.0       3.5
      65.0       1.2
      70.5       1.0
      74.0       1.6
      75.0       2.2
      76.0       1.5
      77.0       3.7
      78.0       1.3
      83.5       3.5
      84.5       4.4
      85.5       4.1
      87.0       1.4
      89.0       2.8
      91.0       1.0
     101.0       1.7
     102.0       2.3
     113.0       1.8
     114.0       1.2
     115.0      24.2
     116.0       2.6
     126.0       4.7
     127.0      13.5
     128.0      25.2
     129.0      11.0
     130.0       4.7
     139.0      14.8
     140.0       4.0
     141.0      80.9
     142.0      64.3
     143.0       7.2
     153.0       2.7
     154.0       7.7
     155.0       2.1
     156.0       3.7
     166.0       1.0
     167.0       2.1
     168.0       7.5
     169.0       3.9
     170.0     100.0
     171.0      86.0
     172.0      10.6

in CDCl3

400 MHz in DMSO-d6

¹H NMR	399.65 MHz
C₁₂ H₁₃ N	0.038 g : 0.5 ml DMSO-d₆
N-methyl-1-naphthalenemethylamine hydrochloride

    Assign.     Shift(ppm)

      A             9.70
      B             8.274
      C     *1      8.02
      D     *1      8.01
      E             7.834
      F             7.63
      G             7.58
      J             7.57
      K             4.630
      L             2.650

     Hz     ppm     Int.

   3877.41   9.703     96
   3310.55   8.284     85
   3303.38   8.266     79
   3302.46   8.264     88
   3208.77   8.029     89
   3206.33   8.023    112
   3205.41   8.021    111
   3201.14   8.010    111
   3199.31   8.006    105
   3197.02   8.000    114
   3135.07   7.845     93
   3134.31   7.843     94
   3128.05   7.827    110
   3062.74   7.664     35
   3061.22   7.660     42
   3055.88   7.647     89
   3054.35   7.643     85
   3052.98   7.640     42
   3047.94   7.627    116
   3047.03   7.625    120
   3045.96   7.622    125
   3045.35   7.621    122
   3040.01   7.607     52
   3038.94   7.605     88
   3037.72   7.601     90
   3032.53   7.588    130
   3030.85   7.584     45
   3025.51   7.571    115
   3024.44   7.568    115
   3017.27   7.550     89
   1850.74   4.631    411
   1059.42   2.651   1000

in CDCl3

in DMSO-d6