65079-19-8

6-氨基-2-甲基喹啉(65079-19-8)核磁圖(¹³CNMR)

產(chǎn)品名稱:6-氨基-2-甲基喹啉

CAS:65079-19-8

分子式:C10H10N2

分子量: 158.2

InChI:InChI=1S/C10H10N2/c1-7-2-3-8-6-9(11)4-5-10(8)12-7/h2-6H,11H2,1H3

InChIKey: TYJFYUVDUUACKX-UHFFFAOYSA-N

Smiles:N1C2C(=CC(N)=CC=2)C=CC=1C

Mass

MS-NW-9583          
2-methyl-6-quinolinamine
C10H10N2            (Mass of molecular ion:    158)

   Source Temperature: 170 °C
   Sample Temperature: 100 °C
   Direct, 75 eV

      18.0       1.6
      28.0       1.1
      51.0       1.6
      52.0       1.3
      63.0       1.6
      64.5       1.1
      65.0       2.3
      66.0       1.6
      77.0       2.7
      78.0       2.2
      79.0       5.3
      89.0       2.4
     102.0       1.0
     103.0       3.6
     104.0       1.5
     115.0       1.0
     116.0       2.5
     117.0       1.0
     128.0       1.1
     130.0      11.3
     131.0       4.5
     132.0       1.1
     140.0       1.5
     141.0       1.1
     142.0       4.1
     143.0       2.4
     155.0       1.9
     156.0       2.0
     157.0      26.6
     158.0     100.0
     159.0      12.0

90 MHz in CDCl3

¹H NMR	89.56 MHz
C₁₀ H₁₀ N₂	0.032 g : 0.5 ml CDCl₃
2-methyl-6-quinolinamine

    Assign.     Shift(ppm)

      A     *1      7.82
      B     *1      7.78
      C             7.148
      D             7.102
      E             6.856
      F             3.9
      G             2.662

     Hz     ppm     Int.

    705.38   7.877    107
    701.25   7.830    101
    696.38   7.776    137
    693.13   7.740    125
    643.81   7.189    187
    641.75   7.166    109
    639.25   7.138    118
    635.44   7.096    140
    632.94   7.068     82
    630.25   7.038    103
    615.13   6.869    153
    612.56   6.840    125
    351.63   3.927     39
    350.25   3.911     40
    349.94   3.908     41
    349.06   3.898     45
    348.75   3.895     43
    348.25   3.889     46
    347.94   3.885     47
    347.19   3.877     47
    346.19   3.866     49
    345.31   3.856     45
    344.50   3.847     45
    343.88   3.840     43
    343.44   3.835     40
    342.75   3.828     38
    342.38   3.823     38
    238.44   2.663   1000

in DMSO-d6