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2815-34-1

反式-2,5-二甲基哌嗪(2815-34-1)紅外圖譜(IR1)

產(chǎn)品名稱:反式-2,5-二甲基哌嗪

CAS:2815-34-1

分子式:C6H14N2

分子量: 114.19

InChI:InChI=1/C6H14N2/c1-5-3-8-6(2)4-7-5/h5-8H,3-4H2,1-2H3/t5-,6+

InChIKey: NSMWYRLQHIXVAP-OLQVQODUNA-N

Smiles:N1C[C@H](C)NC[C@H]1C |&1:2,6,r|

  • 圖譜
    Mass 

    MS-NW-1280          
trans-2,5-dimethylpiperazine
C6H14N2             (Mass of molecular ion:    114)


       Source Temperature: 260 °C
   Sample Temperature: 180 °C
   Reservoir, 75 eV


          15.0       2.1
      18.0       1.5
      27.0       3.3
      28.0      16.8
      29.0       3.1
      30.0      20.5
      32.0       1.1
      39.0       3.6
      41.0      10.2
      42.0      19.9
      43.0       9.6
      44.0      26.5
      54.0       1.5
      55.0       1.1
      56.0      14.6
      57.0       8.1
      58.0     100.0
      59.0       3.7
      68.0       2.0
      70.0      13.9
      71.0       2.8
      83.0       1.1
      84.0       2.8
      85.0       1.0
      99.0      20.7
     100.0       1.3
     113.0       1.5
     114.0       7.2

90 MHz in CDCl3

  • 圖譜

    1H NMR 89.56 MHz
    C6 H14 N2 0.05 g : 0.5 ml CDCl3
    trans-2,5-dimethylpiperazine
    ChemicalStructure 
        Assign.     Shift(ppm)
    
      A             2.94
      B             2.69
      C             2.42
      D             1.61
      E             1.007
  

         Hz     ppm     Int.


        270.56   3.021    107
    268.31   2.996    122
    259.75   2.901    120
    257.63   2.877    186
    239.63   2.676     87
    233.69   2.610     85
    224.25   2.504    241
    214.56   2.396    150
    213.56   2.385    181
    203.88   2.277     83
    143.75   1.606    362
     92.94   1.038   1000
     87.00   0.972    850

in CDCl3

  • 圖譜

CCl4 solution

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KBr disc

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nujol mull

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