2478-10-6

4-羥基丁基丙烯酸酯(2478-10-6)質(zhì)譜(MS)

產(chǎn)品名稱(chēng):4-羥基丁基丙烯酸酯

CAS:2478-10-6

分子式:C7H12O3

分子量: 144.17

InChI:InChI=1S/C7H12O3/c1-2-7(9)10-6-4-3-5-8/h2,8H,1,3-6H2

InChIKey: NDWUBGAGUCISDV-UHFFFAOYSA-N

Smiles:C(OCCCCO)(=O)C=C

Mass

MS-NW-9879          
4-hydroxybutyl acrylate
C7H12O3             (Mass of molecular ion:    144)

   Source Temperature: 270 °C
   Sample Temperature: 150 °C
   Reservoir, 75 eV

      26.0       1.9
      27.0      19.5
      28.0       2.8
      29.0       4.0
      31.0      14.1
      39.0       3.1
      40.0       1.0
      41.0       8.5
      42.0      16.8
      43.0      14.4
      44.0       9.1
      45.0       1.7
      53.0       1.2
      54.0      15.7
      55.0     100.0
      56.0       5.7
      57.0       5.2
      68.0       1.9
      69.0       2.0
      70.0       6.0
      71.0      26.5
      72.0       4.2
      73.0      59.6
      74.0       2.1
      85.0       5.9
      86.0       1.4
      89.0       4.4
      98.0       1.0
      99.0       3.2
     103.0       1.3
     113.0       4.1
     114.0       2.5

400 MHz in CDCl3

¹H NMR	399.65 MHz
C₇ H₁₂ O₃	0.05 ml : 0.5 ml CDCl₃
4-hydroxybutyl acrylate

    Assign.     Shift(ppm)

      A             6.401
      B             6.126
      C             5.843
      D             4.193
      E             3.655
      F             3.09
      G             1.769
      J             1.646

     Hz     ppm     Int.

   2568.85   6.428    328
   2567.38   6.425    329
   2551.51   6.385    445
   2550.05   6.381    437
   2461.43   6.159    384
   2450.93   6.133    457
   2444.09   6.116    284
   2433.59   6.090    342
   2340.70   5.857    428
   2339.23   5.854    411
   2330.32   5.831    350
   2328.74   5.827    351
   1682.37   4.210    555
   1675.78   4.194   1000
   1669.19   4.177    545
   1467.53   3.673    455
   1461.06   3.656    846
   1454.71   3.640    480
   1449.46   3.627     30
   1234.62   3.090     68
    721.44   1.806     75
    720.58   1.804     73
    714.84   1.789    227
    713.99   1.787    223
    710.94   1.779    114
    708.01   1.772    314
    706.91   1.769    267
    704.35   1.763    203
    701.54   1.756    166
    699.58   1.751    294
    692.99   1.734    149
    670.78   1.679    147
    664.92   1.664    300
    664.55   1.663    298
    662.35   1.658    202
    659.67   1.651    223
    656.98   1.644    255
    656.01   1.642    318
    653.20   1.635    111
    650.02   1.627    212
    643.68   1.611     64
    642.58   1.608     65

in CDCl3