四丙基溴化銨(1941-30-6)核磁圖(1HNMR)
分子式:C12H28BrN
分子量: 266.27
InChI:InChI=1S/C12H28N.BrH/c1-5-9-13(10-6-2,11-7-3)12-8-4;/h5-12H2,1-4H3;1H/q+1;/p-1
InChIKey: BGQMOFGZRJUORO-UHFFFAOYSA-M
Smiles:[N+](CCC)(CCC)(CCC)CCC.[Br-]
-
Mass
MS-NW-8191
tetrapropylammonium bromide
C12H28BrN (Mass of molecular ion: 265)
Source Temperature: 200 °C
Sample Temperature: 240 °C
Direct, 75 eV
27.0 12.2
28.0 2.8
29.0 2.0
30.0 17.7
39.0 4.9
40.0 1.0
41.0 20.2
42.0 8.5
43.0 47.2
44.0 4.6
56.0 1.7
58.0 3.3
70.0 2.8
72.0 20.0
80.0 1.0
84.0 2.1
86.0 10.7
100.0 1.3
112.0 1.5
114.0 100.0
115.0 8.2
122.0 3.8
124.0 3.8
142.0 1.4
143.0 7.6
144.0 1.0
186.0 1.5
400 MHz in CDCl3
90 MHz in CDCl3
-
| 1H NMR |
399.65 MHz |
| C12 H28 Br N
|
0.039 g : 0.5 ml CDCl3
|
| tetrapropylammonium bromide
|
 |
Assign. Shift(ppm)
A 3.384
B 1.790
C 1.060
|
Hz ppm Int.
1361.45 3.407 265
1356.45 3.395 166
1352.78 3.385 230
1348.51 3.375 170
1344.24 3.364 293
735.35 1.840 32
728.03 1.822 120
720.58 1.804 177
716.06 1.792 146
711.30 1.780 186
703.74 1.761 137
696.41 1.743 46
430.79 1.078 515
423.58 1.060 1000
416.14 1.042 493
-
| 1H NMR |
89.56 MHz |
| C12 H28 Br N
|
0.048 g : 0.5 ml CDCl3
|
| tetrapropylammonium bromide
|
|
Assign. Shift(ppm)
A 3.38
B 1.78
C 1.07
|
Hz ppm Int.
312.13 3.486 240
307.06 3.429 158
303.81 3.393 204
299.19 3.341 155
295.19 3.297 307
172.69 1.929 103
170.81 1.908 52
165.44 1.848 152
163.38 1.825 110
162.63 1.816 110
160.81 1.796 122
159.63 1.783 111
156.44 1.747 151
148.56 1.659 108
141.69 1.583 43
106.50 1.190 33
101.69 1.136 536
94.69 1.058 1000
87.31 0.975 313
83.75 0.936 31
83.25 0.930 32