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128-09-6

N-氯代丁二酰亞胺(128-09-6)質(zhì)譜(MS)

產(chǎn)品名稱:N-氯代丁二酰亞胺

CAS:128-09-6

分子式:C4H4ClNO2

分子量: 133.53

InChI:InChI=1S/C4H4ClNO2/c5-6-3(7)1-2-4(6)8/h1-2H2

InChIKey: JRNVZBWKYDBUCA-UHFFFAOYSA-N

Smiles:N1(Cl)C(=O)CCC1=O

  • 圖譜
    Mass 

    MS-NW-8724          
N-chlorosuccinimide
C4H4ClNO2           (Mass of molecular ion:    133)


       Source Temperature: 140 °C
   Sample Temperature: 100 °C
   Direct, 75 eV


          14.0       1.6
      15.0       1.6
      26.0       5.4
      27.0      11.5
      28.0      78.6
      29.0       2.6
      36.0       4.0
      38.0       1.5
      42.0      16.2
      43.0       2.1
      44.0       1.5
      49.0       1.1
      54.0       1.1
      55.0      56.9
      56.0      50.9
      57.0       1.8
      70.0      23.2
      77.0       2.8
      80.0       7.8
      98.0      19.3
      99.0       5.7
     100.0       1.4
     105.0      11.5
     107.0       3.8
     133.0     100.0
     134.0       7.3
     135.0      32.5
     136.0       2.3

400 MHz in DMSO-d6

  • 圖譜

    1H NMR 399.65 MHz
    C4 H4 Cl N O2 0.038 g : 0.5 ml DMSO-d6
    N-chlorosuccinimide
    ChemicalStructure 
        Assign.     Shift(ppm)
    
      A             2.573
  

         Hz     ppm     Int.


       1082.52   2.709     33
   1036.38   2.594     24
   1028.56   2.574   1000
   1019.29   2.551     24
    970.83   2.430     22

DMSO-d6

  • 圖譜

KBr disc

  • 圖譜

nujol mull

  • 圖譜

4880 A,200 M,powder

  • 圖譜

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